Building materials are required for a wide range of construction work including carpentry, roofing, structural reinforcement, insulation, and plumbing. The particle size and particle shape of the raw materials influence quality and performance of the end product, and therefore require quality control by particle characterization. Microtrac analyzers are successfully used to determine the size and shape of various building materials.
Building materials range from naturally occurring substances such as rock, clay, sand, and wood to synthetic polymers and multiple combinations of both (composites). Concrete or mortar are for example mixtures of cement and aggregates like sand or gravel.
Le CAMSIZER X2 est un analyseur de particules puissant et extrêmement polyvalent, doté d'une large gamme de mesure qui combine une technologie de caméra de pointe et des options de dispersion flexibles. Basé sur le principe de l'analyse dynamique des images (ISO 13322-2), le CAMSIZER X2 fournit des informations précises sur la taille et la forme des particules de poudres, de granulés et de suspensions dans une plage de mesure allant de 0,8 μm à 8 mm.
Le CAMSIZER X2 produit un flux de particules qui est caractérisé par un système optique à haute résolution. Une source lumineuse stroboscopique à LED ultra-lumineuses et deux caméras numériques haute résolution permettent d'obtenir une fréquence d'images de plus de 300 images par seconde qui sont évaluées en temps réel par un logiciel puissant. Ainsi, le CAMSIZER X2 capture les images de centaines de milliers à plusieurs millions de particules avec une précision maximale en seulement 1 à 3 minutes.
Le CAMSIZER X2 fournit une large sélection d'informations sur les particules, ce qui permet une caractérisation complète et fiable de l'échantillon de matériau. Il est adapté à une utilisation en R&D ainsi qu'à des tâches de routine dans le cadre du contrôle qualité.
In most cases the particle size distribution of sand used in building materials is analyzed by sieve analysis. Microtrac's CAMSIZER series can replace this time-consuming and error-prone technique with a quicker, more reliable method that provides a higher resolution of particle size results as well as additional particle shape information.
Deux types de sable prélevés à différents endroits, mesurés avec le CAMSIZER X2. Ce sable est utilisé comme couche dans les tuyaux en plastique renforcé de verre pour en augmenter la rigidité. Le paramètre de taille indiqué est xc min (= largeur des particules). La courbe rouge est légèrement bimodale. Le sable avec une large distribution de taille peut être plus étroitement tassé au cœur du tuyau, ce qui confère au produit fini une plus grande stabilité.
One sand sample that was measured by sieving (black) and by the CAMSIZER X2 using two different dispersion modules: the X-Fall module (green) and the X-Jet module (red). The results compare extremely well, proving that CAMSIZER X2 can match existing sieve analysis results. Hence, product specifications based on sieve analysis can remain unchanged when transitioning to a CAMSIZER system.
Limestone (calcium carbonate) is a raw material used in many products.
The particle size distribution as measured with the CAMSIZER X2 for a range of limestone grades.
The particle shape distribution results for the same collection of limestone samples. The reported shape parameter is sphericity, defined as: sphericity = 4 p A/ P2 where "A = Area of the particle projection" and "P = Perimeter length of the particle projection". The least round sample is Nr 6 (red), while the most round sample is Nr 4 (light blue).
Typical result from a particle size analysis of a plaster sample. The size range is fairly wide, ranging from 2 microns to about 1 mm. The graph shows the result of the CAMSIZER X2 in X-Jet mode, measured with a dispersion pressure of 150 kPa (red curve).
The plaster particles are agglomerating and “sticky”, thus the results of a conventional sieve analysis shows much coarser data (black curve), especially for the fine particles. However, if the particles are dispersed properly with an air jet sieve (AS 200 jet, blue curve), the results agree perfectly with the CAMSIZER X2.
Save and reliable detection of oversized particles are among the most important objectives of particle size analyis. For this purpose, Dynamic Image Analysis with the CAMSIZER X2 is the most powerful technique with unmatched accuracy.
Figure 6 shows a silicate sample that was analyzed with the CAMSIZER X2 using the X-Fall module. First, the original sample was measured and the size distribution was found to range from 5 μm to 100 μm (red curve). Then, 0.1 % of oversized (> 100 μm) particles were added and the sample was analyzed again (green curve). Finally, the experiment was repeated with 1 % oversize added (blue curve).
This silicate is used as raw material for the coating of tiles and oversized particles will result in a rough and uneven surface of the finished tile. The CAMSIZER X2 reliably detects the correct amount of oversize. Note that below 100 μm, where all samples are identical, the reproducibility is excellent!